TA Instruments

AR1756-0015f

15/03/2013 15:18:35

Sample name	ASW Blank coupon#20 + DI + beads 250rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	15 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:18:35

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 250.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	249.5	-5366.8	10000	20.0	0.4535	1.004	-1749	311.9	-5.608	1848	260.5430	0.01899	325.68	32568	3.411E-3	0.0	0.0
2.0160	250.0	494.62	10000	20.0	0.4230	2.016	161.2	312.5	0.5160	1724	459.1600	0.01765	573.95	57395	3.411E-3	0.0	0.0
3.0160	250.0	511.85	10000	20.0	0.4236	3.016	166.8	312.4	0.5340	1726	761.7840	0.01768	952.23	95223	3.411E-3	0.1	0.1
4.0160	250.0	506.30	10000	20.0	0.4184	4.016	165.0	312.5	0.5281	1705	961.6510	0.01745	1202.1	1.2021E5	3.411E-3	0.1	0.1
5.0120	250.0	489.70	10000	20.0	0.4222	5.012	159.6	312.5	0.5108	1720	1162.9100	0.01761	1453.6	1.4536E5	3.411E-3	0.1	0.1
6.0160	250.0	491.02	10000	20.0	0.4230	6.016	160.0	312.5	0.5121	1724	1464.5500	0.01765	1830.7	1.8307E5	3.411E-3	0.1	0.1
7.0160	250.0	482.14	10000	20.0	0.4216	7.016	157.2	312.5	0.5029	1718	1666.9600	0.01759	2083.7	2.0837E5	3.411E-3	0.1	0.1
8.0160	250.0	481.88	10000	20.0	0.4216	8.016	157.1	312.5	0.5026	1718	1968.9900	0.01759	2461.2	2.4612E5	3.411E-3	0.1	0.1
8.9960	250.0	493.96	10000	20.0	0.4171	8.996	161.0	312.5	0.5152	1700	2168.0601	0.01741	2710.1	2.7101E5	3.411E-3	0.1	0.1
10.016	250.0	470.05	10000	20.0	0.4240	10.016	153.2	312.5	0.4903	1728	2469.7900	0.01769	3087.2	3.0872E5	3.411E-3	0.2	0.2
11.016	250.0	483.25	10000	20.0	0.4263	11.016	157.5	312.5	0.5040	1737	2681.5400	0.01778	3351.9	3.3519E5	3.411E-3	0.2	0.2
12.016	250.0	494.19	10000	20.0	0.4208	12.016	161.1	312.5	0.5154	1714	2972.2500	0.01755	3715.3	3.7153E5	3.411E-3	0.2	0.2
13.016	250.0	477.60	10000	20.0	0.4212	13.016	155.7	312.5	0.4982	1716	3173.4199	0.01757	3966.8	3.9668E5	3.411E-3	0.2	0.2
14.016	250.0	473.44	10000	20.0	0.4234	14.016	154.3	312.5	0.4938	1725	3475.0100	0.01767	4343.8	4.3438E5	3.411E-3	0.2	0.2
15.016	250.0	491.29	10000	20.0	0.4178	15.016	160.1	312.5	0.5124	1702	3677.0300	0.01743	4596.3	4.5963E5	3.411E-3	0.3	0.3
16.020	250.0	476.05	10000	20.0	0.4305	16.020	155.2	312.5	0.4965	1754	3977.5200	0.01796	4971.9	4.9719E5	3.411E-3	0.3	0.3
17.024	250.0	482.83	10000	20.0	0.4293	17.024	157.4	312.5	0.5036	1749	4178.7402	0.01791	5223.4	5.2234E5	3.411E-3	0.3	0.3
18.016	250.0	470.56	10000	20.0	0.4322	18.016	153.4	312.5	0.4908	1761	4482.6001	0.01803	5603.3	5.6033E5	3.411E-3	0.3	0.3
19.016	250.0	478.30	10000	20.0	0.4216	19.016	155.9	312.5	0.4989	1718	4681.2700	0.01759	5851.6	5.8516E5	3.411E-3	0.3	0.3
20.016	250.0	482.04	10000	20.0	0.4224	20.016	157.1	312.5	0.5028	1721	4983.9800	0.01762	6230.0	6.2300E5	3.411E-3	0.3	0.3
21.016	250.0	489.94	10000	20.0	0.4178	21.016	159.7	312.5	0.5110	1702	5186.0498	0.01743	6482.6	6.4826E5	3.411E-3	0.4	0.4
22.020	250.0	478.74	10000	20.0	0.4212	22.020	156.0	312.5	0.4993	1716	5488.7700	0.01757	6861.0	6.8610E5	3.411E-3	0.4	0.4
23.016	250.0	482.58	10000	20.0	0.4238	23.016	157.3	312.5	0.5034	1727	5686.5498	0.01769	7108.2	7.1082E5	3.411E-3	0.4	0.4
24.012	250.0	476.84	10000	20.0	0.4141	24.012	155.4	312.5	0.4973	1687	5989.2900	0.01727	7486.6	7.4866E5	3.411E-3	0.4	0.4
25.016	250.0	482.82	10000	20.0	0.4196	25.016	157.4	312.5	0.5036	1710	6190.4702	0.01750	7738.1	7.7381E5	3.411E-3	0.4	0.4
26.016	250.0	481.33	10000	20.0	0.4234	26.016	156.9	312.5	0.5020	1725	6492.1602	0.01766	8115.2	8.1152E5	3.411E-3	0.4	0.4
27.008	250.0	472.81	10000	20.0	0.4155	27.008	154.1	312.5	0.4931	1693	6691.8101	0.01733	8364.8	8.3648E5	3.411E-3	0.5	0.5
28.064	250.0	469.07	10000	20.0	0.4293	28.064	152.9	312.5	0.4892	1749	6996.9199	0.01791	8746.2	8.7462E5	3.411E-3	0.5	0.5
29.016	250.0	490.23	10000	20.0	0.4153	29.016	159.8	312.5	0.5114	1692	7194.5498	0.01733	8993.2	8.9932E5	3.411E-3	0.5	0.5
30.024	250.0	485.78	10000	20.0	0.4214	30.024	158.3	312.5	0.5067	1717	7498.6001	0.01758	9373.3	9.3733E5	3.411E-3	0.5	0.5
31.016	250.0	474.06	10000	20.0	0.4212	31.016	154.5	312.5	0.4945	1716	7697.2500	0.01757	9621.6	9.6216E5	3.411E-3	0.5	0.5
32.020	250.0	480.69	10000	20.0	0.4188	32.020	156.7	312.5	0.5014	1706	7999.7402	0.01747	9999.7	9.9997E5	3.411E-3	0.5	0.5
33.020	250.0	484.25	10000	20.0	0.4169	33.020	157.8	312.5	0.5051	1699	8200.8799	0.01739	10251	1.0251E6	3.411E-3	0.6	0.6
34.016	250.0	481.33	10000	20.0	0.4218	34.016	156.9	312.5	0.5020	1719	8502.2900	0.01759	10628	1.0628E6	3.411E-3	0.6	0.6
35.016	250.0	487.41	10000	20.0	0.4182	35.016	158.9	312.5	0.5084	1704	8702.5098	0.01745	10878	1.0878E6	3.411E-3	0.6	0.6
36.016	250.0	483.22	10000	20.0	0.4226	36.016	157.5	312.5	0.5041	1722	9010.0303	0.01764	11263	1.1263E6	3.411E-3	0.6	0.6
37.016	250.0	478.12	10000	20.0	0.4220	37.016	155.8	312.5	0.4987	1719	9205.5703	0.01761	11507	1.1507E6	3.411E-3	0.6	0.6
38.024	250.0	482.86	10000	20.0	0.4234	38.024	157.4	312.5	0.5036	1725	9510.7500	0.01767	11888	1.1888E6	3.411E-3	0.6	0.6
39.012	250.0	480.28	10000	20.0	0.4180	39.012	156.5	312.5	0.5009	1703	9707.7803	0.01744	12135	1.2135E6	3.411E-3	0.7	0.7
40.016	250.0	490.91	10000	20.0	0.4129	40.016	160.0	312.5	0.5121	1682	10011.200	0.01723	12514	1.2514E6	3.411E-3	0.7	0.7
41.024	250.0	473.15	10000	20.0	0.4188	41.024	154.2	312.5	0.4936	1706	10212.500	0.01747	12766	1.2766E6	3.411E-3	0.7	0.7
42.032	250.0	491.68	10000	20.0	0.4192	42.032	160.3	312.5	0.5129	1708	10516.700	0.01749	13146	1.3146E6	3.411E-3	0.7	0.7
43.012	250.0	477.08	10000	20.0	0.4141	43.012	155.5	312.5	0.4976	1687	10714.200	0.01728	13393	1.3393E6	3.411E-3	0.7	0.7
44.016	250.0	483.83	10000	20.0	0.4115	44.016	157.7	312.5	0.5047	1676	10915.100	0.01717	13644	1.3644E6	3.411E-3	0.7	0.7
45.020	250.0	476.06	10000	20.0	0.4149	45.020	155.2	312.5	0.4965	1691	11217.000	0.01731	14021	1.4021E6	3.411E-3	0.8	0.8
46.012	250.0	489.75	10000	20.0	0.4145	46.012	159.6	312.5	0.5108	1689	11416.600	0.01729	14271	1.4271E6	3.411E-3	0.8	0.8
47.016	250.0	476.22	10000	20.0	0.4107	47.016	155.2	312.5	0.4967	1673	11718.200	0.01713	14648	1.4648E6	3.411E-3	0.8	0.8
48.004	250.0	482.82	10000	20.0	0.4151	48.004	157.4	312.5	0.5036	1691	11921.200	0.01732	14902	1.4902E6	3.411E-3	0.8	0.8
49.016	250.0	484.99	10000	20.0	0.4196	49.016	158.1	312.5	0.5058	1710	12221.000	0.01750	15276	1.5276E6	3.411E-3	0.8	0.8
50.020	250.0	483.25	10000	20.0	0.4115	50.020	157.5	312.5	0.5041	1676	12422.000	0.01717	15528	1.5528E6	3.411E-3	0.8	0.8
51.016	250.0	476.93	10000	20.0	0.4133	51.016	155.5	312.5	0.4975	1684	12734.800	0.01724	15919	1.5919E6	3.411E-3	0.9	0.9
52.016	250.0	485.40	10000	20.0	0.4143	52.016	158.2	312.5	0.5063	1688	12925.800	0.01729	16157	1.6157E6	3.411E-3	0.9	0.9
53.016	250.0	479.44	10000	20.0	0.4127	53.016	156.3	312.5	0.5000	1681	13226.300	0.01722	16533	1.6533E6	3.411E-3	0.9	0.9
54.016	250.0	491.96	10000	20.0	0.4111	54.016	160.4	312.5	0.5131	1675	13427.200	0.01715	16784	1.6784E6	3.411E-3	0.9	0.9
55.020	250.0	479.67	10000	20.0	0.4157	55.020	156.3	312.5	0.5003	1694	13728.800	0.01734	17161	1.7161E6	3.411E-3	0.9	0.9
56.012	250.0	477.71	10000	20.0	0.4204	56.012	155.7	312.5	0.4982	1713	13929.800	0.01754	17412	1.7412E6	3.411E-3	0.9	0.9
57.016	250.0	478.46	10000	20.0	0.4204	57.016	156.0	312.5	0.4990	1713	14232.500	0.01754	17791	1.7791E6	3.411E-3	1.0	1.0
58.020	250.0	495.81	10000	20.0	0.4121	58.020	161.6	312.5	0.5171	1679	14432.500	0.01719	18041	1.8041E6	3.411E-3	1.0	1.0
59.020	250.0	501.18	10000	20.0	0.4171	59.020	163.4	312.5	0.5228	1700	14735.300	0.01741	18419	1.8419E6	3.411E-3	1.0	1.0
60.016	250.0	470.08	10000	20.0	0.4157	60.016	153.2	312.5	0.4903	1694	14935.300	0.01734	18669	1.8669E6	3.411E-3	1.0	1.0

